;noesyesgpph ;avance-version (12/01/11) ;2D homonuclear correlation via dipolar coupling ;dipolar coupling may be due to noe or chemical exchange. ;phase sensitive ;water suppression using excitation sculpting with gradients ; ;T.-L. Hwang & A.J. Shaka, J. Magn. Reson., ; Series A 112 275-279 (1995) ; ;$CLASS=HighRes ;$DIM=2D ;$TYPE= ;$SUBTYPE= ;$COMMENT= prosol relations= #include #include #include "p2=p1*2" "d11=30m" "d12=20u" "in0=inf1" "d0=in0/2-p1*4/3.1416" "TAU=de+p1*2/3.1416+54u" "acqt0=0" baseopt_echo 1 ze 4u pl19:f2 2 d1 cw:f2 ph29 3 d12 pl1:f1 do:f2 p1 ph1 d0 p1 ph2 d8 cw:f2 ph29 4u do:f2 p1 ph3 50u UNBLKGRAD p16:gp1 d16 pl0:f1 (p12:sp1 ph4:r):f1 4u d12 pl1:f1 p2 ph5 4u p16:gp1 d16 TAU p16:gp2 d16 pl0:f1 (p12:sp1 ph6:r):f1 4u d12 pl1:f1 p2 ph7 4u p16:gp2 d16 4u BLKGRAD go=2 ph31 d1 mc #0 to 2 F1PH(calph(ph1, +90), caldel(d0, +in0)) exit ph1= 0 0 2 2 ph2= 0 ph3= 0 0 0 0 2 2 2 2 1 1 1 1 3 3 3 3 ph4= 0 0 0 0 1 1 1 1 ph5= 2 2 2 2 3 3 3 3 ph6= 2 3 ph7= 0 1 ph29=0 0 0 0 0 0 0 0 1 1 1 1 1 1 1 1 ph31=0 2 2 0 0 2 2 0 1 3 3 1 1 3 3 1 ;pl0 : 0W ;pl1 : f1 channel - power level for pulse (default) ;sp1 : f1 channel - shaped pulse 180 degree ;p1 : f1 channel - 90 degree high power pulse ;p2 : f1 channel - 180 degree high power pulse ;p12: f1 channel - 180 degree shaped pulse (Squa100.1000) [2 msec] ;p16: homospoil/gradient pulse ;d0 : incremented delay (2D) ;d1 : relaxation delay; 1-5 * T1 ;d8 : mixing time ;d12: delay for power switching [20 usec] ;d16: delay for homospoil/gradient recovery ;inf1: 1/SW = 2 * DW ;in0: 1/(1 * SW) = 2 * DW ;nd0: 1 ;ns: 8 * n ;ds: 16 ;td1: number of experiments ;FnMODE: States-TPPI, TPPI, States or QSEQ ;use gradient ratio: gp 1 : gp 2 ; 31 : 11 ;for z-only gradients: ;gpz1: 31% ;gpz2: 11% ;use gradient files: ;gpnam1: SMSQ10.100 ;gpnam2: SMSQ10.100 ;Processing ;PHC0(F1): 90 ;PHC1(F1): -180 ;FCOR(F1): 1 ;$Id: noesyesgpph,v 1.11.6.1 2012/01/31 17:56:34 ber Exp $